Sodium octanoate synthesis
- Product Name:Sodium octanoate
- CAS Number:1984-06-1
- Molecular formula:C8H15NaO2
- Molecular Weight:166.19
Yield:-
Reaction Conditions:
with sodium hydroxide in 2-ethoxy-ethanol;5,5-dimethyl-1,3-cyclohexadiene;water;
Steps:
2 Reaction of sodium caprylate with 2-chloroethanol
Sodium caprylate (2 mol) was prepared by neutralization of caprylic acid (2 mol; 288,4 g; 317, 4 ml) in 750 ml of xylene with sodium hydroxide (2 mol; 80 g) in water (160 ml). The reaction mixture was freed of water and then heated with chloroethanol (2,1 mol; 170 g; 204,4 ml) with addition of 2-ethoxyethanol (1000 ml) as a solvent under reflux for 28 hours. The precipitated NaCl was filtered off and washed with 2-ethoxyethanol.
References:
EP316918,1990,A3
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