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ChemicalBook CAS DataBase List 2-Octyl-1-dodecanol
5333-42-6

2-Octyl-1-dodecanol synthesis

9synthesis methods
2-Octyl-1-dodecanol is produced by the condensation of two molecules of decyl alcohol. It also occurs naturally in small quantities in plants.
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Yield:5333-42-6 90%

Reaction Conditions:

with sodium hydroxide

Steps:

1 EXAMPLE 1

EXAMPLE 1 To 967 g. of decylalcohol in a 2 liter 4-necked glass reaction flask, 30 g. of sodium hydroxide and 2.0 g. of nickel were added during agitation. The mixture was heated to 230°-250° C. and stirred for 6 hours while water of reaction was removed by distillation. The contents of the reactor was then allowed to cool and product, 2-decyl-decan-1-ol, was recovered in greater than 90% yield. The product, purified by distillation, was identified by gas liquid partition chromatography (GLC).

References:

US4830769,1989,A

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