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ChemicalBook CAS DataBase List 2-BUTYL-1-OCTANOL
3913-02-8

2-BUTYL-1-OCTANOL synthesis

7synthesis methods
-

Yield:3913-02-8 86%

Reaction Conditions:

with zinc(II) oxide;sodium hydroxide at 210; for 3 h;Inert atmosphere;Temperature;

Steps:

1.1; 2.1; 3.1; 4.1; 5.1 Example 3
(1) Add 204g n-hexanol, 10.2g sodium hydroxide, and 1.13g zinc oxide to the reaction kettle connected to the water separator. The reaction kettle replaces nitrogen and under the protection of nitrogen, slowly raises the temperature to 210 ° C and reacts for 3h. After filtration and distillation, 160 g of isododecyl alcohol was obtained.

References:

Zhejiang Lvke'an Chemical Co., Ltd.;Zhejiang Huangma Technology Co., Ltd.;Jiang Xuefeng;Wan Qingmei;Wu Yongjun;Chen Tiejun CN110981906, 2020, A Location in patent:Paragraph 0019; 0022; 0025; 0028; 0031; 0036-0037

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