(S)-5-HYDROXYMETHYL TOLTERODINE synthesis
- Product Name:(S)-5-HYDROXYMETHYL TOLTERODINE
- CAS Number:260389-90-0
- Molecular formula:C22H31NO2
- Molecular Weight:341.49
94-02-0
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260389-90-0
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Yield:-
Steps:
Multi-step reaction with 6 steps
1: sodium tetrahydroborate / methanol / 0.5 h / Cooling with ice; Inert atmosphere
2: 3 h / Inert atmosphere
3: 24 h / Reflux; Inert atmosphere
4: perchloric acid / dichloromethane; water / 13 h / 40 °C / Inert atmosphere
5: sodium tetrahydroborate; calcium chloride / ethanol / 3 h / -10 - 20 °C / Inert atmosphere
6: tert-Amyl alcohol / 17 h / 20 - 70 °C / Inert atmosphere
References:
Lee, Youngeun;Shabbir, Saira;Jeong, Yuri;Ban, Jaeyoung;Rhee, Hakjune [Bulletin of the Korean Chemical Society,2015,vol. 36,# 12,p. 2885 - 2889]
4850-49-1
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260389-90-0
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290362-27-5
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260389-90-0
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1055330-27-2
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![3-[bis(propan-2-yl)amino]-1-phenylpropan-1-ol](/CAS/20200119/GIF/906532-26-1.gif)
906532-26-1
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260389-90-0
34 suppliers
$195.00/1mg