O-Mesitylenesulfonylhydroxylamine synthesis
- Product Name:O-Mesitylenesulfonylhydroxylamine
- CAS Number:36016-40-7
- Molecular formula:C9H13NO3S
- Molecular Weight:215.27
36016-39-4
97 suppliers
$19.00/250mg
36016-40-7
138 suppliers
inquiry
Yield:36016-40-7 100%
Reaction Conditions:
with trifluoroacetic acid at 0; for 1.5 h;
Steps:
Amino 2,4,6-trimethylbenzenesulfonate
TFA (10 mL) was cooled to ice temperature, then Intermediate] (5.0 g, 15.87 mmol) was added. The reaction mixture was stirred at 0°C for 1.5 h, then poured onto crushed ice. The resulting white-coloured precipitate was filtered off, then washed with water (100 mL) and dried under vacuum, to obtain the title compound (4.1 g, quantitative) as a white solid. This material was taken though to the next step without any purification.0H (400 MHz, CDC13) 6.99 (s, 2H), 5.48 (s, 2H), 2.68 (s, 6H), 2.32 (s, 3H).
References:
WO2015/86502,2015,A1 Location in patent:Page/Page column 81
38202-27-6
160 suppliers
$6.00/1g
36016-40-7
138 suppliers
inquiry
![Ethanimidic acid, N-[[(2,4,6-trimethylphenyl)sulfonyl]oxy]-, ethyl ester, (1E)-](/CAS/20210111/GIF/1239506-69-4.gif)
1239506-69-4
0 suppliers
inquiry
36016-40-7
138 suppliers
inquiry
773-64-8
266 suppliers
$5.00/5g
36016-40-7
138 suppliers
inquiry
58658-55-2
0 suppliers
inquiry
36016-40-7
138 suppliers
inquiry