N,N-Diethylcyanoacetamide synthesis
- Product Name:N,N-Diethylcyanoacetamide
- CAS Number:3010-02-4
- Molecular formula:C6H12N2
- Molecular Weight:112.17
109-89-7
465 suppliers
$10.00/5g
590-17-0
328 suppliers
$5.00/5g
3010-02-4
79 suppliers
$138.00/25mL
Yield: 90%
Reaction Conditions:
in ethyl acetate
Steps:
S.21 Synthesis of diethylaminoacetonitrile (Amine 21)
Synthesis Example 21 Synthesis of diethylaminoacetonitrile (Amine 21) At 0° C., 12.0 g of bromoacetonitrile was added to 14.6 g of diethylamine. The mixture was heated to 20° C. over 10 hours. Ethyl acetate was added to the reaction mixture, and the resulting solids were filtered off. Distillation yielded diethylaminoacetonitrile (boiling point: 170° C., yield: 90%). IR (thin film): ν=2976, 2222, 1461, 1389, 1322, 1206, 1093, 984 cm-1 13C-NMR (75 MHz in CDCl3): δ=12.6, 40.5, 47.9, 114.8
References:
Shin-Etsu Chemical Co., Ltd. US6743564, 2004, B2
102588-37-4
0 suppliers
inquiry
3010-02-4
79 suppliers
$138.00/25mL
50-00-0
864 suppliers
$10.00/25g
3010-02-4
79 suppliers
$138.00/25mL
107-14-2
283 suppliers
$15.00/25g
109-89-7
465 suppliers
$10.00/5g
3010-02-4
79 suppliers
$138.00/25mL
