Ethyl cyclopropanecarboxylate synthesis
- Product Name:Ethyl cyclopropanecarboxylate
- CAS Number:4606-07-9
- Molecular formula:C6H10O2
- Molecular Weight:114.14
1759-53-1
469 suppliers
$6.00/10g
4606-07-9
145 suppliers
$10.00/1g
Yield:4606-07-9 98%
Reaction Conditions:
with sulfuric acid in ethanol;
Steps:
9 EXAMPLE 9
EXAMPLE 9 To a 10-mL, three-necked flask equipped with a condenser, a magnetic stir bar and a thermometer is charged cyclopropanecarboxylic acid (8.6 g), ethanol (23 mL) and 2 drops of concentrated sulfuric acid. The mixture is refluxed (approximately 85° C.) for 16 hours. GC analysis shows that 98% of the cyclopropanecarboxylic acid has been consumed and a 98% yield of ethyl cyclopropanecarboxylate is obtained.
References:
US5504245,1996,A
3153-36-4
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$14.00/25mL
4606-07-9
145 suppliers
$10.00/1g
64-17-5
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$10.00/50g
1759-53-1
469 suppliers
$6.00/10g
4606-07-9
145 suppliers
$10.00/1g
623-73-4
149 suppliers
$27.30/25ML
115-11-7
235 suppliers
$45.00/25g
4606-07-9
145 suppliers
$10.00/1g
623-73-4
149 suppliers
$27.30/25ML
74-85-1
104 suppliers
$79.00/11l
4606-07-9
145 suppliers
$10.00/1g