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ChemicalBook CAS DataBase List Ethyl 4-amino-1-piperidinecarboxylate
58859-46-4

Ethyl 4-amino-1-piperidinecarboxylate synthesis

1synthesis methods
29976-53-2 Synthesis
N-Carbethoxy-4-piperidone

29976-53-2
388 suppliers
$5.00/5g

-

Yield: 93%

Reaction Conditions:

Stage #1:N-ethoxycarbonyl-4-piperidone with titanium(IV) isopropylate;ammonia in ethanol at 25; for 6 h;
Stage #2: with sodium tetrahydroborate in ethanol at 25; for 3 h;Further stages.;

References:

Miriyala, Bruhaspathy;Bhattacharyya, Sukanta;Williamson, John S. [Tetrahedron,2004,vol. 60,# 7,p. 1463 - 1471]

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