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ChemicalBook CAS DataBase List ETHYL 2-METHYL-4-PHENYL-1,3-THIAZOLE-5-CARBOXYLATE
32043-95-1

ETHYL 2-METHYL-4-PHENYL-1,3-THIAZOLE-5-CARBOXYLATE synthesis

2synthesis methods
-

Yield:-

Reaction Conditions:

Stage #1: ethyl 3-oxo-3-phenylpropionatewith hydroxy(phenyl)-λ3-iodanyl 2,4-dinitrobenzenesulfonate in acetonitrile at 120; for 0.00833333 h;
Stage #2: thioacetamide in acetonitrile; for 0.0166667 h;Microwave irradiation;

References:

Choi, Min Jeong;No, Eun Sun;Thorat, Dhanaji Achyutrao;Jang, Jae Wan;Yang, Hakkyun;Lee, Jaeick;Choo, Hyunah;Kim, Soo Jin;Lee, Chang Sik;Ko, Soo Young;Lee, Jiyoun;Nam, Ghilsoo;Pae, Ae Nim [Journal of Medicinal Chemistry,2013,vol. 56,# 22,p. 9008 - 9018]

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