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ChemicalBook CAS DataBase List Butanedihydrazide
4146-43-4

Butanedihydrazide synthesis

7synthesis methods
-

Yield:4146-43-4 65%

Reaction Conditions:

with hydrazine hydrate in ethanol for 12 h;Reflux;

Steps:

Succinyl hydrazide
Succinyl hydrazide was synthesised following a literaturepreparation [44]. Diethyl succinate (2.8 mL, 17 mmol)and hydrazine monohydrate (4.2 mL, 85 mmol) wereadded sequentially to ethanol (10 mL) and the solutionwas heated at re;ux for 12 hours during which a whitecrystalline precipitate formed. After cooling to roomtemperature, the white precipitate was

References:

Kruger, Paul E.;Wilson, Benjamin H. [Supramolecular Chemistry,2020,p. 1 - 10]

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