Acetamiprid synthesis
- Product Name:Acetamiprid
- CAS Number:135410-20-7
- Molecular formula:C10H11ClN4
- Molecular Weight:222.67
1558-82-3
135 suppliers
$10.00/5g
![N-[(6-CHLOROPYRIDIN-3-YL)METHYL]-N-METHYLAMINE](/CAS/GIF/120739-62-0.gif)
120739-62-0
63 suppliers
$56.00/100mg
135410-20-7
420 suppliers
$24.00/10mg
Yield:135410-20-7 96.6%
Reaction Conditions:
in ethanol at 65;
Steps:
3 Example 3
Preparation of acetamiprid
(500 ml) was added 157.5 g of N- (6-chloro-3-pyridylmethyl) methylamine and 100 g of ethanol,Further, 112 g of cyanoethyl ester,Heated to 65 ° C,Insulation reaction 6 to 7 hours,At the end of the reaction,Cooled to 0 ° C,Standing stratification,filter,Washed with saturated brine,After drying,Acetamidine 22.1 g,Purity 96.8%Yield 96.6%.
References:
CN106187868,2016,A Location in patent:Paragraph 0015