2-Piperidineethanol synthesis
- Product Name:2-Piperidineethanol
- CAS Number:1484-84-0
- Molecular formula:C7H15NO
- Molecular Weight:129.2
110-89-4
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1484-84-0
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Yield:-
Steps:
Multi-step reaction with 4 steps
1: 30 percent / H2O2, sodium tungstate dihydrate / methanol / under 5 deg C, then Rt, 24 h
2: CH2Cl2 / 12 h / Heating
3: 94 percent / LiAlH4 / tetrahydrofuran / 0 deg C, then reflux, 3 h
4: ammonium formate, 10percent Pd/C / methanol / 12 h / Heating
References:
Carruthers, William;Moses, Roger C. [Journal of the Chemical Society. Perkin transactions I,1988,p. 2251 - 2254]