2-Phenylthiopyridine synthesis
15synthesis methods
- Product Name:2-Phenylthiopyridine
- CAS Number:3111-54-4
- Molecular formula:C11H9NS
- Molecular Weight:187.26
Yield:3111-54-4 97%
Reaction Conditions:
with 1.2.3.4-tetrahydro-8-hydroxy-quinoline;Cs2CO3;copper(II) bromide in N,N-dimethyl-formamide at 130; for 48 h;Inert atmosphere;chemoselective reaction;
References:
Li, Yaming;Li, Xiaoying;Wang, Huifeng;Chen, Tao;Xie, Yusheng [Synthesis,2010,# 21,art. no. F10410SS,p. 3602 - 3608] Location in patent:supporting information; experimental part