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ChemicalBook CAS DataBase List 2,4,6,8,10,12-HEXAMETHYLCYCLOHEXASILOXANE, 96
6166-87-6

2,4,6,8,10,12-HEXAMETHYLCYCLOHEXASILOXANE, 96 synthesis

5synthesis methods
-

Yield:2370-88-9 35.6% ，6166-86-5 16.7% ，6166-87-6 4.4%

Reaction Conditions:

with H2O in diethyl ether;water;addn. of (CH3)SiHCl2 to a mixt. of ether and crushed ice at -10 to 7°C under vigorous stirring;;

References:

Sauer, O.;Scheiber, W. J.;Brewer, S. D. [Journal of the American Chemical Society,1946,vol. 68,p. 962 - 963] [Gmelin Handbuch der Anorganischen Chemie,Gmelin Handbook: Si: MVol.C, 99, page 271 - 274]