1-Methylpiperidin-4-amine synthesis
- Product Name:1-Methylpiperidin-4-amine
- CAS Number:41838-46-4
- Molecular formula:C6H14N2
- Molecular Weight:114.19
1445-73-4
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41838-46-4
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Yield:41838-46-4 100%
Reaction Conditions:
with ammonium formate;palladium on carbon in methanol;
Steps:
25.3A.1
Step: 3A-1Synthesis of l-Methyl-piperidin-4-yIamineProcedure:Ammonium formate (2.226g, 0.035348mol) was added to a solution of 1 -Methyl- piperidin-4-one (lg, 0.008837mol) in MeOH and stirred for lOmins. 20% Pd-C was added to this and the reaction mixture was heated at 60°C for 2hrs. The reaction was monitored by the TLC (10% methanol in chloroform). The reaction mixture was filtered through celite bed, concentrated to afford lg (100% yield) of l-Methyl-piperidin-4-ylamine.
References:
WO2012/59932,2012,A1 Location in patent:Page/Page column 137
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65220-86-2
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41838-46-4
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