Succimer synthesis
1synthesis methods
- Product Name:Succimer
- CAS Number:304-55-2
- Molecular formula:C4H6O4S2
- Molecular Weight:182.22
Isolate
the solid complexes of trivalent lanthanide complexes with
meso-2,3-Dimercaptosuccinic Acid, furan-2-carboxylic acid,
meso-2,3-dimercaptosuccinic acid and sarcosine from the mixture of
equimolar solutions of metal nitrates and ligands. Adjust the pH of the
mixture to 7 by adding dilute solution of KOH. Reflux the mixture in
ethanol (15-20 ml) for 3-4 hours on a steam bath. The clear solution
gives a solid mass on cooling, filter through G4 glass crucible and wash
several times with the mixture of doubly distilled water and alcohol.
Recrystallise it to obtain pure crystal and dry at 60 ° -70 °C [1].
53318-26-6
0 suppliers
inquiry
304-55-2
338 suppliers
$8.00/1g
Yield:-
Reaction Conditions:
with sodium hydroxide
References:
Gerecke,M. et al. [Helvetica Chimica Acta,1961,vol. 44,p. 955 - 960]