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ChemicalBook--->CAS DataBase List--->5332-24-1

5332-24-1

5332-24-1 Structure

5332-24-1 Structure
IdentificationMore
[Name]

3-Bromoquinoline
[CAS]

5332-24-1
[Synonyms]

3-BROMOQUINLIINE
3-BROMOQUINOLINE
3-bromo-quinolin
3-Bromoquinoline98%Or99%
3-Bromoquinoline 98 %
Bromoquinoline
Quinoline, 3-bromo-
3-Bromoquinoline ,98% [HPLC 98%]
[EINECS(EC#)]

226-237-1
[Molecular Formula]

C9H6BrN
[MDL Number]

MFCD00006767
[Molecular Weight]

208.05
[MOL File]

5332-24-1.mol
Chemical PropertiesBack Directory
[Appearance]

colorless to light yellow liquid
[Melting point ]

13-15 °C (lit.)
[Boiling point ]

274-276 °C (lit.)
[density ]

1.533 g/mL at 25 °C(lit.)
[vapor pressure ]

0.196Pa at 25℃
[refractive index ]

n20/D 1.664(lit.)
[Fp ]

>230 °F
[storage temp. ]

Keep Cold
[form ]

Liquid
[pka]

2.69(at 25℃)
[color ]

Clear colorless to yellow
[Water Solubility ]

103mg/L at 25℃
[Detection Methods]

GC,NMR
[BRN ]

112939
[InChIKey]

ZGIKWINFUGEQEO-UHFFFAOYSA-N
[CAS DataBase Reference]

5332-24-1(CAS DataBase Reference)
[NIST Chemistry Reference]

Quinoline, 3-bromo-(5332-24-1)
[EPA Substance Registry System]

5332-24-1(EPA Substance)
Safety DataBack Directory
[Hazard Codes ]

Xi
[Risk Statements ]

R36/37/38:Irritating to eyes, respiratory system and skin .
[Safety Statements ]

S26:In case of contact with eyes, rinse immediately with plenty of water and seek medical advice .
S36:Wear suitable protective clothing .
S37/39:Wear suitable gloves and eye/face protection .
[RIDADR ]

UN2810
[WGK Germany ]

3
[TSCA ]

Yes
[HS Code ]

29334900
Raw materials And Preparation ProductsBack Directory
[Raw materials]

1-Benzoyl-1,2-dihydro-2-quinolinecarbonitrile-->3-Bromoquinoline-1-oxide-->3,6-DIBROMOQUINOLINE-->QUINOLINE HYDROCHLORIDE-->3-Quinolinecarboxylic acid-->2-Bromomalonaldehyde
[Preparation Products]

5-Aminonicotinic acid-->3-Quinolinecarboxaldehyde-->3-Quinolineboronic acid-->3-Aminoquinoline-->3-BROMOQUINOLINE-8-SULFONIC ACID-->1-QUINOLIN-3-YLETHANONE-->N-(propan-2-yl)quinolin-3-amine-->4-(3-QUINOLINYL)BENZONITRILE
Material Safety Data Sheet(MSDS)Back Directory
[msds information]

3-Bromoquinoline(5332-24-1).msds
Hazard InformationBack Directory
[Chemical Properties]

colorless to light yellow liquid
[Synthesis Reference(s)]

The Journal of Organic Chemistry, 27, p. 1318, 1962 DOI: 10.1021/jo01051a047
[General Description]

3-Bromoquinoline undergoes bromine-magnesium exchange reaction with lithium tributylmagnesate in toluene at -10°C, which is quenched by various electrophiles to yield functionalized quinolines.
[Flammability and Explosibility]

Notclassified
Questions And AnswerBack Directory
[Bromoquinoline]

There are seven position isomers with the main properties are as follows:
Name
Melting point(℃)
Boiling point(℃)
Solubility
2-bromoquinoline
48~49
It is soluble in diethyl ether, chloroform and benzene
3-bromoquinoline
12~15
274~276, 95(66.66Pa)
4-bromoquinoline
29~30
270(decomposition)
Easily soluble in dilute acid
5-bromoquinoline
52 (needle crystal)
280
6-bromoquinoline
24
278
7-bromoquinoline
52 (needle crystal)
290
8-bromoquinoline
80
165~166
(2399.79Pa)
[Application and synthesis method]

3-Bromoquinoline can have action with mixed acid to generate 3-bromo-5-nitroquinoline, followed by heating with potassium permanganate to be oxidized to 5-bromo-2, 3-pyridine dicarboxylic acid.
6-bromo-quinoline can be heated together nitric acid to generate 6-bromo-8-nitro-quinoline, followed by reaction with potassium permanganate to be oxidized into 2, 3-pyridinedicarboxylic acid.
2-bromo-quinoline can be manufactured through the reaction between 2-hydroxyquinoline and phosphorus pentabromide
3-bromo-quinoline can be obtained through heating the quinoline perbromide at 180 ° C.
4-bromoquinoline can be obtained through either the heating reaction between 4-hydroxyquinoline and phosphorus pentabromide or by the diazotization reaction of 4-aminoquinoline.
5-bromo-quinoline can be obtained from the heating reaction between m-bromo aniline, glycerol, m-bromonitrobenzene and concentrated sulfuric acid, or through the diazotization reaction of 5-amino-quinoline.
6-bromo-quinoline can be obtained through the heating reaction between p-bromoaniline, glycerol, concentrated sulfuric acid and p-bromo-nitrobenzene.
7-bromoquinoline can be obtained through the diazotization of 7-aminoquinoline.
8-bromo-quinoline can be obtained through the heating of o-bromo aniline, glycerol, concentrated sulfuric acid and o-bromo-nitrobenzene in the heating system.
Purposes: as organic synthesis reagents.
[Uses]

For pharmaceuticals
Medicine, pesticide intermediates
Spectrum DetailBack Directory
[Spectrum Detail]

3-Bromoquinoline(5332-24-1)MS
3-Bromoquinoline(5332-24-1)1HNMR
3-Bromoquinoline(5332-24-1)13CNMR
3-Bromoquinoline(5332-24-1)IR1
3-Bromoquinoline(5332-24-1)Raman
Well-known Reagent Company Product InformationBack Directory
[Acros Organics]

3-Bromoquinoline, 98%(5332-24-1)
[Alfa Aesar]

3-Bromoquinoline, 98%(5332-24-1)
[Sigma Aldrich]

5332-24-1(sigmaaldrich)
[TCI AMERICA]

3-Bromoquinoline,>98.0%(GC)(T)(5332-24-1)
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