TRIETHYL 3-PHOSPHONOPROPIONATE synthesis
- Product Name:TRIETHYL 3-PHOSPHONOPROPIONATE
- CAS Number:3699-67-0
- Molecular formula:C9H19O5P
- Molecular Weight:238.22
41978-69-2
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3699-67-0
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Yield:3699-67-0 93%
Reaction Conditions:
with triethyl phosphite
Steps:
1 EXAMPLE 1
EXAMPLE 1 Triethyl Phosphonopropionate: Ethyl bromopropionate (92 g 0.5 mole) and triethyl phosphite (83 g, 0.5 mole) were stirred and heated to about 200° C. under a air cooled reflux condenser. The ethyl bromide that was evolved was collected with the aid of a cooling trap. After 1 hour of heating the pot temperature went up to 230° C. At this point the evolution of ethyl bromide ceased. The yellow oil was cooled to room temperature (RT) and then distilled under vacuum. There was obtained 112 g of phosphonate (93%) boiling at 105° /20 mm Hg as a colorless oil.
References:
US5162566,1992,A
762-04-9
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140-88-5
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3699-67-0
96 suppliers
$21.00/1g
