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ChemicalBook CAS DataBase List tert-butyl 4-methylphenyl ether
15359-98-5

tert-butyl 4-methylphenyl ether synthesis

9synthesis methods
-

Yield:-

Steps:

Multi-step reaction with 2 steps
1.1: hydrogenchloride; sodium nitrite / water / 0.75 h / 0 - 5 °C
1.2: 1 h
2.1: boron trifluoride diethyl etherate / 0.17 h / 110 °C / Inert atmosphere; Microwave irradiation

References:

Kovac, Mitja;Anderluh, Marko;Vercouillie, Johnny;Guilloteau, Denis;Emond, Patrick;Mavel, Sylvie [Journal of Fluorine Chemistry,2013,vol. 147,p. 5 - 9]

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