SODIUM METHACRYLATE synthesis
- Product Name:SODIUM METHACRYLATE
- CAS Number:5536-61-8
- Molecular formula:C4H5NaO2
- Molecular Weight:108.07
79-41-4
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$14.00/5g
5536-61-8
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Yield:5536-61-8 92.2%
Reaction Conditions:
with sodium hydroxide in water;acetone
Steps:
2 Example 2
Example 2 Preparation of Sodium Methacrylate A 12.23 g (0.3058 mol) sample of sodium hydroxide was placed in a 50-ml Erlenmayer flask equipped with 10 ml water and a magnetic stirring bar, and the mixture was stirred to dissolution. The sodium hydroxide solution was then poured into a 250-ml beaker containing 30.70 g (0.3570 mol) methacrylic acid (exothermic reaction) with constant stirring. The mixture was allowed to cool, 50 ml of acetone were added, and the precipitate vacuum filtered. The recovered carboxylate salt was first allowed to air dry under a hood, and then dried in an oven at 55°-60° C. for 12-15 hours to afford 30.43 g (92.2% yield) of sodium methacrylate.
References:
Howard University US5491244, 1996, A
760-93-0
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71-00-1
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5536-61-8
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$6.00/10g
13282-13-8
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