RARECHEM AL BW 0442 synthesis
- Product Name:RARECHEM AL BW 0442
- CAS Number:56622-54-9
- Molecular formula:C7H10N2
- Molecular Weight:122.17
3222-48-8
200 suppliers
$16.00/1 g
56622-54-9
67 suppliers
$52.00/100mg
Yield:56622-54-9 90%
Reaction Conditions:
with ammonia;hydrogen in methanol at 20; for 2 h;
Steps:
12 Preparation of (6-methylpyridin-3-yl) methanamine
Procedure H: To a mixture of 6-methylnicotinonitrile (300 mg, 2.54 mmol) in MeOH/NH3 (7N, 10mL), was added Raney Ni (50 mg). The reaction mixture was stirred at RT for 3 h under H2. It was then filtered, and the filtrate concentrated in vacuo to give 6- methylpyridin-3-yl) methanamine as a yellow oil (280 mg, 90%). LC-MS (ESI): m/z (M+1)+ = 123.30.
References:
REMEDY PLAN, INC.;CRIMMINS, Gregory, Thomas;DE JESúS DIAZ, Dennise, Alexandra;BHURRUTH-ALCOR, Yushma WO2019/213570, 2019, A1 Location in patent:Paragraph 0331; 0402-0404
6960-22-1
162 suppliers
$39.00/1g
56622-54-9
67 suppliers
$52.00/100mg
474554-80-8
2 suppliers
inquiry
56622-54-9
67 suppliers
$52.00/100mg
28900-10-9
239 suppliers
$9.00/1g
56622-54-9
67 suppliers
$52.00/100mg
4241-27-4
214 suppliers
$6.00/250mg
56622-54-9
67 suppliers
$52.00/100mg