RARECHEM AL BI 0214 synthesis
1synthesis methods
- Product Name:RARECHEM AL BI 0214
- CAS Number:708-25-8
- Molecular formula:C9H8F2O2
- Molecular Weight:186.16
Yield:-
Reaction Conditions:
with sulfuric acidReflux;
Steps:
General procedure for synthesis of benzohydrazidederivatives (4a-m):
General procedure: To a stirred solution of different benzoic acids (6.42 mmol) in ethanol (3 mL) was added H2SO4 (0.1mL) and heated to reflux for 6-10 h. The reaction mixture was diluted with ethyl acetate followed by water. The organic layer was washed with saturated NaHCO3 followed by water and brine solution. The organic layer was dried over sodium sulphate, filtered and evaporated to obtain the respective ethyl benzoate derivatives.
References:
Prasanna, V. Laxmi;Narender [Asian Journal of Chemistry,2015,vol. 27,# 10,p. 3605 - 3608]