N-(2-HYDROXYETHYL)-2,2,2-TRIFLUOROACETAMIDE synthesis
- Product Name:N-(2-HYDROXYETHYL)-2,2,2-TRIFLUOROACETAMIDE
- CAS Number:6974-29-4
- Molecular formula:C4H6F3NO2
- Molecular Weight:157.09
Yield:-
Reaction Conditions:
at 0 - 20;
Steps:
1.1.d 2,2,2-trifluoro-N-(2-hydroxyethyl)acetamide (IX)
Ethanolamine (8.5 mL, 141 mmol) was cooled to 0° C. Trifluoro acetic acid (22.3 mL, 289 mmol) was added dropwise. The reaction mixture was allowed to warm up to room temperature. The product precipitates as a white solid
References:
IMEC VZW;UNIVERSITEIT HASSELT;Lutsen, Laurence;Vanderzande, Dirk US2020/152395, 2020, A1 Location in patent:Paragraph 0219; 0221
141-43-5
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6974-29-4
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6974-29-4
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6974-29-4
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141-43-5
903 suppliers
$9.00/10g
6974-29-4
45 suppliers
$144.00/25ml