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ChemicalBook CAS DataBase List Menthyl isovalerate
16409-46-4

Menthyl isovalerate synthesis

3synthesis methods
Prepared by heating a mixture of l-menthol and isovaleric acid at 100 to 110°C in the presence of trace concentrated H2SO4 or at 100°C in the presence of HCl.
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Yield: 99.7%

Reaction Conditions:

with palladium diacetate;hydrogen;toluene-4-sulfonic acid;triphenylphosphine in xylene at 100; under 13680 Torr; for 2 h;

References:

Suerbayev, Kh.A.;Tsukanov, I.A.;El'man, A.R.;Zhubanov, K.A. [Russian Journal of General Chemistry,1994,vol. 64,# 7.2,p. 1072 - 1074][Zhurnal Obshchei Khimii,1994,vol. 64,# 7,p. 1189 - 1191]

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