ChemicalBook CAS DataBase List ethyl(2-naphthyl)amine

ethyl(2-naphthyl)amine synthesis

13synthesis methods

Product Name:ethyl(2-naphthyl)amine
CAS Number:2437-03-8
Molecular formula:C12H13N
Molecular Weight:171.24

101-02-0 Synthesis

101-02-0
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75-04-7
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$10.00/20mg

135-19-3 Synthesis

135-19-3
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$9.00/1g

2437-03-8
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Yield:2437-03-8 96%

Reaction Conditions:

in water;

Steps:

32 N-ethyl-β-naphthylamine

EXAMPLE 32 N-ethyl-β-naphthylamine 288 parts of β-naphthol, 6.6 parts of triphenyl phosphite and 115 parts of ethylamine gas are heated for 10 hours at 230° C in a pressure autoclave. The pressure is 35 atmospheres. The mixture is added to 2,000 parts of water and the batch is stirred for 30 minutes at 70° - 80° C. The lower oily phase is separated off and distilled. 328 parts of N-ethyl-β-naphthylamine of boiling point 119° - 120° C/0.1 mm Hg are obtained. This corresponds to a yield of 96% of theory.

References:

US4067903,1978,A

75-04-7
393 suppliers
$10.00/20mg

135-19-3 Synthesis

135-19-3
739 suppliers
$9.00/1g

2437-03-8
24 suppliers
inquiry

References