ChemicalBook CAS DataBase List Dipropyl succinate

Dipropyl succinate synthesis

7synthesis methods

Product Name:Dipropyl succinate
CAS Number:925-15-5
Molecular formula:C10H18O4
Molecular Weight:202.25

Dipropyl succinate is produced by direct esterification of n-Propanol with Succinic acid e. g. under azeotropic conditions.

71-23-8 Synthesis

71-23-8
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$12.00/100g

110-15-6 Synthesis

110-15-6
960 suppliers
$5.00/10g

925-15-5
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$35.29/10g

Yield: 97%

Reaction Conditions:

with alumina methanesulfonic acid at 80; for 0.133333 h;Microwave irradiation;

Steps:

Representative Procedure for Preparation of Aromatic and Aliphatic Esters (Table 1)
General procedure: In a typical reaction, AMA 2:3 (332 g, 0.6 mol), the corresponding carboxylicacid (1 mol), and alcohol (1.5-2 mol) were mixed in the provided reaction glass tubeequipped with a screw cap and magnetic agitation until a wet mixture was achieved.The reaction mixture was irradiated with microwaves (Anton Parr Monowave 300reactor) at 80 C for 8 min or 120 C for 20 min. On cooling, the mixture was diluted with dichloromethane (41 mL), filtered under gravity, and washed with dichloromethane;then the filtrate was washed with Na2CO3 (ss) and water. The organic layerwas dried over Na2SO4, filtered, and concentrated under reduced pressure to give theester.

References:

Fabian, Lucas;Gomez, Matias;Kuran, Juan A. Caturelli;Moltrasio, Graciela;Moglioni, Albertina [Synthetic Communications,2014,vol. 44,# 16,p. 2386 - 2392]

71-23-8 Synthesis

71-23-8
759 suppliers
$12.00/100g

645-67-0 Synthesis