Allylmagnesium chloride synthesis
- Product Name:Allylmagnesium chloride
- CAS Number:2622-05-1
- Molecular formula:C3H5ClMg
- Molecular Weight:100.83
75-54-7
176 suppliers
$32.47/25G
107-05-1
418 suppliers
$16.80/100ML
2622-05-1
155 suppliers
$40.00/500mg
Yield:-
Reaction Conditions:
with magnesium in tetrahydrofuran
Steps:
R.5 Synthesis of diallylmethylchlorosilane
REFERENCE EXAMPLE 5 Synthesis of diallylmethylchlorosilane Allylmagnesium chloride was synthesised by the gradual dropwise addition of 50 parts of allyl chloride to a mixture of 15 parts of magnesium turnings and 100 parts of tetrahydrofuran. This was gradually added dropwise over a period of 2 hours to 18 parts of methyldichlorosilane dissolved in 100 parts of tetrahydrofuran, and the reaction was then heated for an additional 1 hour under reflux.
References:
Dow Corning Asia, Ltd. US5502229, 1996, A
107-05-1
418 suppliers
$16.80/100ML
2622-05-1
155 suppliers
$40.00/500mg
7439-95-4
0 suppliers
$11.60/0.9g
107-05-1
418 suppliers
$16.80/100ML
2622-05-1
155 suppliers
$40.00/500mg
107-05-1
418 suppliers
$16.80/100ML
187737-37-7
1 suppliers
inquiry
592-42-7
181 suppliers
$22.00/25mL
613-12-7
79 suppliers
$203.00/1g
2622-05-1
155 suppliers
$40.00/500mg