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ChemicalBook CAS DataBase List 7-Bromo-3,4-dihydro-2H-benzo[1,4]oxazine
105679-22-9

7-Bromo-3,4-dihydro-2H-benzo[1,4]oxazine synthesis

5synthesis methods
27684-84-0 Synthesis
PHENOL, 5-BROMO-2-NITRO-

27684-84-0
152 suppliers
$9.00/1g

-

Yield:-

Steps:

Multi-step reaction with 3 steps
1: iron; ammonium chloride / ethanol; water / 0.5 h / 50 - 70 °C
2: caesium carbonate / acetonitrile / 20 °C
3: borane-THF / tetrahydrofuran / 1 h / Inert atmosphere; Reflux

References:

Lv, Yongcong;Li, Mengyuan;Liu, Ting;Tong, Linjiang;Peng, Ting;Wei, Lixin;Ding, Jian;Xie, Hua;Duan, Wenhu [ACS Medicinal Chemistry Letters,2014,vol. 5,# 5,p. 592 - 597]

FullText

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