6-NITROISOQUINOLINE synthesis
- Product Name:6-NITROISOQUINOLINE
- CAS Number:70538-57-7
- Molecular formula:C9H6N2O2
- Molecular Weight:174.16
3470-54-0
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Yield:-
Steps:
Multi-step reaction with 4 steps
1: 56 percent / pertrifluoroacetic acid / CH2Cl2 / 13 h / Ambient temperature
2: sodium borohydride / methanol / 3 h / Ambient temperature
3: 82 percent / p-Toluenesulfonic acid / benzene / 3 h / Heating
References:
Miller, R. Bryan;Frincke, James M. [Journal of Organic Chemistry,1980,vol. 45,# 26,p. 5312 - 5315]
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