(6-ETHOXYPYRIDIN-3-YL)BORONIC ACID synthesis
- Product Name:(6-ETHOXYPYRIDIN-3-YL)BORONIC ACID
- CAS Number:612845-44-0
- Molecular formula:C7H10BNO3
- Molecular Weight:166.97
55849-30-4
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$12.72/1gm:
612845-44-0
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$6.00/250mg
Yield: 61%
Reaction Conditions:
Stage #1:5-bromo-2-ethoxypyridine with n-butyllithium in diethyl ether;hexane at -78; for 2 h;
Stage #2: with Triisopropyl borate in diethyl ether;hexane at -78; for 2 h;
References:
Parry, Paul R.;Bryce, Martin R.;Tarbit, Brian [Synthesis,2003,# 7,p. 1035 - 1038]