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ChemicalBook CAS DataBase List 6-Chloro-4-methyl-7-azaindole
4894-29-5

6-Chloro-4-methyl-7-azaindole synthesis

2synthesis methods
-

Yield:-

Steps:

Multi-step reaction with 3 steps
1: palladium (II) [1,1'-bis(diphenylphosphanyl)ferrocene] dichloride / tetrahydrofuran; toluene / 5 h / 0 - 80 °C / Inert atmosphere
2: 3-chloro-benzenecarboperoxoic acid / dichloromethane / 4 h / 0 - 20 °C
3: 1,1,1,3,3,3-hexamethyl-disilazane; methyl chloroformate / tetrahydrofuran / 1.5 h / 0 - 20 °C

References:

WO2022/184130,2022,A1

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