5-IODO-1-METHYL-1H-PYRAZOLE synthesis
- Product Name:5-IODO-1-METHYL-1H-PYRAZOLE
- CAS Number:34091-51-5
- Molecular formula:C4H5IN2
- Molecular Weight:208
930-36-9
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34091-51-5
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Yield: 92%
Reaction Conditions:
Stage #1:1-methyl-1H-pyrazole with (PMDETA)2K2Mg(CH2SiMe3)4 at 0; for 2 h;Inert atmosphere;Schlenk technique;
Stage #2: with iodine for 1 h;Inert atmosphere;Schlenk technique;regioselective reaction;
References:
Baillie, Sharon E.;Bluemke, Tobias D.;Clegg, William;Kennedy, Alan R.;Klett, Jan;Russo, Luca;De Tullio, Marco;Hevia, Eva [Chemical Communications,2014,vol. 50,# 85,p. 12859 - 12862] Location in patent:supporting information
930-36-9
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$5.00/1g
![Ethanamine, N-[(3,5-dichlorophenyl)methylene]-2,2-diethoxy-](/CAS/20210305/GIF/1000210-73-0.gif)
1000210-73-0
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1000210-73-0
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34091-51-5
109 suppliers
$15.00/1g