4-Chloro-3-fluorophenol synthesis
- Product Name:4-Chloro-3-fluorophenol
- CAS Number:348-60-7
- Molecular formula:C6H4ClFO
- Molecular Weight:146.55
137504-86-0
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348-60-7
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Yield:348-60-7 > 99 %Spectr.
Reaction Conditions:
with oxygen;triethylamine in acetonitrile; under 760.051 Torr; for 4 h;Irradiation;
Steps:
2.3. Photocatalytic hydroxylation of phenylboronic acid
General procedure: The photocatalytic hydroxylation of phenylboronic acid wascarried out as following: Catalyst (10 mg) and phenylboronicacid (0.5 mmol) was poured into the mixture solution with triethylamine (TEA, 1.5 mmol) dissolved in the acetonitrile (3 mL).Then, the mixture was transferred into a 10 mL Pyrex glass bottlefilled with pure oxygen at atmospheric pressure. The suspensionswere irradiated by a blue LED lamp. After the reaction, the mixturewas centrifuged to completely remove the catalyst particles. Thefiltered solution was analyzed by 1H NMR spectrum using 1, 3, 5-Trimethoxybenzene as the internal standard.
References:
Anpo, Masakazu;Cheng, Jiajia;Huang, Caijin;Ou, Honghui;Ren, Wei;Wang, Xinchen [Journal of Catalysis,2020,vol. 389,p. 636 - 645]
![Benzene, 1-chloro-2-fluoro-4-[2-(trimethylsilyl)ethoxy]-](/CAS/20210305/GIF/1338215-43-2.gif)
1338215-43-2
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348-60-7
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170793-00-7
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348-60-7
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367-22-6
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348-60-7
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