4-Biphenylacetonitrile synthesis
- Product Name:4-Biphenylacetonitrile
- CAS Number:31603-77-7
- Molecular formula:C14H11N
- Molecular Weight:193.24
773837-37-9
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Yield: 173.7 g
Reaction Conditions:
in water at 70 - 75; for 4 h;Time;
Steps:
3
1000 ml four bottles into the 500g water,182.2 g Biphenyl monochlorobenzyl chloride,44.1 g of sodium cyanide,Heating to 70 ~ 75 between the incubation reaction 4 hours,Cooled to room temperature and filtered to give 173.7 g of 4-biphenylacetonitrile,Water is treated with hydrogen peroxide.
References:
Huangshi Lifuda Pharmaceutical Chemical Co., Ltd.;Cheng, Jiagang CN106431911, 2017, A Location in patent:Paragraph 0063; 0066; 0073; 0080
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