4-(2-METHOXYETHOXY)ANILINE synthesis
- Product Name:4-(2-METHOXYETHOXY)ANILINE
- CAS Number:33311-29-4
- Molecular formula:C9H13NO2
- Molecular Weight:167.21
109-86-4
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$11.00/25g
350-46-9
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33311-29-4
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$46.00/1 g
Yield: 76.9%
Reaction Conditions:
with dimethyl sulfoxide;potassium hydroxide at 60;
Steps:
7 Synthesis of intermediate 4- (2-methoxyethoxy) aniline
P-fluoronitrobenzene (0.5g, 3.54mmol),Ethylene glycol methyl ether (0.335ml, 4.25mmol), potassium hydroxide (0.3g, 5.31mmol) was added to 10ml of dimethyl sulfoxide, stirred at 60 overnight, water analysis, suction filtration0.537 g of a yellow solid was obtained with a yield of 76.9%.
References:
China Pharmaceutical University;Xiang Hua;Teng Yu;Li Zhenbang;Xiao Maoxu;Ren Shengnan;Ha Si;Tong Chao CN111057021, 2020, A Location in patent:Paragraph 0088-0090
22483-40-5
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$7.00/250mg
33311-29-4
72 suppliers
$46.00/1 g
109-86-4
541 suppliers
$11.00/25g
540-37-4
444 suppliers
$6.00/5g
33311-29-4
72 suppliers
$46.00/1 g
350-46-9
515 suppliers
$10.60/1gm:
33311-29-4
72 suppliers
$46.00/1 g