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ChemicalBook CAS DataBase List 3-METHYLBENZYL ISOCYANATE
61924-25-2

3-METHYLBENZYL ISOCYANATE synthesis

3synthesis methods
-

Yield:-

Steps:

Multi-step reaction with 3 steps
1: oxalyl chloride, dimethylformamide / CH2Cl2 / 0.42 h
2: NaN3 / acetone; H2O / 0.5 h / 0 - 5 °C
3: CHCl3 / 0.5 h / Heating

References:

Shah, Shrenik K.;Dorn, Conrad P.;Finke, Paul E.;Hale, Jeffrey J.;Hagmann, William K.;et al. [Journal of Medicinal Chemistry,1992,vol. 35,# 21,p. 3745 - 3754]

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