天堂网亚洲,天天操天天搞,91视频高清,菠萝蜜视频在线观看入口,美女视频性感美女视频,95丝袜美女视频国产,超高清美女视频图片

Welcome to chemicalbook!
Chinese English Japanese Germany Korea
400-158-6606
Try our best to find the right business for you.
Do not miss inquiry messages Please log in to view all inquiry messages.

Welcome back!

ChemicalBook CAS DataBase List 2'-HYDROXY-4',6'-DIMETHOXYACETOPHENONE
90-24-4

2'-HYDROXY-4',6'-DIMETHOXYACETOPHENONE synthesis

13synthesis methods
Preparation by reaction of acetonitrile on phloroglucinol dimethyl ether (Hoesch reaction).
-

Yield:90-24-4 100%

Reaction Conditions:

with potassium carbonate in acetone for 3 h;Reflux;

Steps:


To a refluxing solution of 2,4,6-trihydroacetophenone-monohydrate (10 g, 53.7 mmol) and K2CO3 (15 g, 108.7 mmol) in acetone (150 mL), (CH3)2SO4 was added at three hour intervals (3 x 3.5 mL, 40.0 mmol). The solution was filtered and the solvent was evaporated to afford 2,4-dimethoxy-6-hydroxyacetophenone as a yellow solid (98%).

References:

UNIVERSITY OF LOUISVILLE RESEARCH FOUNDATION, INC.;UNIVERSIDAD PERUMA CAYETANO HEREDIA;INSTITUT DE RECHERCHE POUR LE DEVELOPPEMENT (IRD);THE JOHNS HOPKINS UNIVERSITY;HAMMOND, Gerald, B.;APONTE, Jose, C.;GILMAN, Robert, H.;SAUVAIN, Michel, Henri-Auguste;VAISBERG, Abraham WO2010/19861, 2010, A1 Location in patent:Page/Page column 38; 50

FullText

2'-HYDROXY-4',6'-DIMETHOXYACETOPHENONE Related Search: