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ChemicalBook CAS DataBase List 2-BROMO-5-CHLOROBENZOIC ACID ETHYL ESTER
690260-91-4

2-BROMO-5-CHLOROBENZOIC ACID ETHYL ESTER synthesis

2synthesis methods
-

Yield:690260-91-4 66%

Reaction Conditions:

with sodium persulfate;N-Bromosuccinimide;trifluorormethanesulfonic acid;palladium diacetate in 1,2-dichloro-ethane at 90; for 5 h;Sealed tube;regioselective reaction;

References:

Sun, Xiuyun;Shan, Gang;Sun, Yonghui;Rao, Yu [Angewandte Chemie - International Edition,2013,vol. 52,# 16,p. 4440 - 4444][Angew. Chem.,2013,vol. 125,# 16,p. 4536 - 4540,5] Location in patent:supporting information

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