1-ACENAPHTHENOL synthesis
- Product Name:1-ACENAPHTHENOL
- CAS Number:6306-07-6
- Molecular formula:C12H10O
- Molecular Weight:170.21
2235-15-6
129 suppliers
$100.00/1 g
6306-07-6
92 suppliers
$26.50/1g
Yield: 94.2%
Reaction Conditions:
with hydrogen in methanol at 100; under 30003 Torr;Autoclave;Temperature;
Steps:
2.1
1) In a 1000 ml autoclave, 700 ml of methanol was added as a solvent,Followed by the addition of 168 gl-acenaphthene, 13 g hydrogenation catalyst nickel catalyst AMG-1200; added to complete, sealed reactor,First use the nitrogen to replace the kettle air twice, through the H2 to the pressure4.OMPa, open the stirring, heating to 100 ° C to react, the reaction to no hydrogen,1-naphthenaphthene was removed and the reaction was stopped,Followed by column purification of 1 - hydroxy acenaphthalene pure product 160.14g, the yield was 94.2%
References:
Wang Jiju CN106397116, 2017, A Location in patent:Paragraph 0012
83-32-9
266 suppliers
$14.00/5g
6306-07-6
92 suppliers
$26.50/1g
2235-15-6
129 suppliers
$100.00/1 g
208-96-8
263 suppliers
$5.00/250mg
6306-07-6
92 suppliers
$26.50/1g
83-32-9
266 suppliers
$14.00/5g
6306-07-6
92 suppliers
$26.50/1g
82-86-0
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$10.00/1g
191-48-0
70 suppliers
$500.13/5MG
6306-07-6
92 suppliers
$26.50/1g
83-32-9
266 suppliers
$14.00/5g
208-96-8
263 suppliers
$5.00/250mg