2-氯-6-硝基苯甲醛(6361-22-4)質(zhì)譜(MS)

產(chǎn)品名稱:2-氯-6-硝基苯甲醛

CAS:6361-22-4

分子式:C7H4ClNO3

分子量: 185.56

Mass

MS-IW-0240          
2-chloro-6-nitrobenzaldehyde
C7H4ClNO3           (Mass of molecular ion:    185)

   Source Temperature: 260 °C
   Sample Temperature: 160 °C
   Reservoir, 75 eV

      18.0       1.8
      28.0       2.7
      29.0       2.8
      30.0       5.1
      36.0       1.0
      37.0       2.7
      38.0       2.1
      39.0       3.2
      44.0       1.1
      49.0       2.1
      50.0      11.8
      51.0       6.6
      61.0       2.9
      62.0       2.7
      63.0      10.6
      64.0       1.9
      73.0      12.9
      74.0      15.8
      75.0      72.7
      76.0       9.7
      77.0       1.4
      78.0       2.7
      84.0       4.3
      85.0       5.0
      86.0       2.3
      87.0       2.4
      90.0       1.3
      91.0      28.7
      92.0       4.8
      99.0      79.3
     100.0       4.7
     101.0      25.7
     102.0       1.5
     109.0       1.1
     110.0      27.5
     111.0      10.5
     112.0       9.6
     113.0       3.7
     126.0       2.6
     127.0       4.5
     128.0       1.1
     129.0       1.4
     138.0      25.6
     139.0       2.4
     140.0       8.2
     155.0     100.0
     156.0       8.0
     157.0      32.3
     158.0       2.5
     168.0       2.4

400 MHz in CDCl3

¹H NMR	399.65 MHz
C₇ H₄ Cl N O₃	0.038 g : 0.5 ml CDCl₃
2-chloro-6-nitrobenzaldehyde

    Assign.     Shift(ppm)

      A            10.376
      B             7.977
      C             7.771
      D             7.642

     Hz     ppm     Int.

   4147.03  10.377   1000
   3192.75   7.989    280
   3191.99   7.987    281
   3184.51   7.969    314
   3183.90   7.967    308
   3111.11   7.785    300
   3110.05   7.782    294
   3106.84   7.774     33
   3105.77   7.772     36
   3103.03   7.765    412
   3101.96   7.762    378
   3061.52   7.661    405
   3053.44   7.641    631
   3047.64   7.626     26
   3045.20   7.620    267

in CDCl3