二烯丙基胺鹽酸鹽(6147-66-6)核磁圖(¹HNMR)

產(chǎn)品名稱:二烯丙基胺鹽酸鹽

CAS:6147-66-6

分子式:C6H12ClN

分子量: 133.62

InChI:InChI=1S/C6H11N.ClH/c1-3-5-7-6-4-2;/h3-4,7H,1-2,5-6H2;1H

InChIKey: PZNOBXVHZYGUEX-UHFFFAOYSA-N

Smiles:N(CC=C)CC=C.Cl

¹HNMR

IR1

IR2

Mass

MS-IW-3078          
diallylamine hydrochloride
C6H11N HCl          (Mass of molecular ion:     97)

   Source Temperature: 150 °C
   Sample Temperature: 110 °C
   Direct, 75 eV

      15.0       2.8
      17.0       1.4
      18.0       5.9
      26.0       3.6
      27.0      11.0
      28.0      45.5
      29.0       5.7
      30.0      18.5
      35.0       9.7
      36.0      68.1
      37.0       3.7
      38.0      23.4
      39.0      47.1
      40.0       6.1
      41.0      99.2
      42.0      21.3
      43.0      13.3
      44.0       1.3
      52.0       2.5
      53.0       2.2
      54.0      16.7
      55.0       9.9
      56.0      32.7
      57.0       2.3
      65.0       1.3
      67.0       8.3
      68.0      88.3
      69.0      12.8
      70.0     100.0
      71.0       5.6
      77.0       1.5
      79.0       3.5
      80.0       7.8
      81.0       6.8
      82.0      66.8
      83.0       4.0
      94.0       5.1
      96.0      35.0
      97.0      40.8
      98.0       3.0

90 MHz in CDCl3

¹H NMR	89.56 MHz
C₆ H₁₁ N	0.047 g : 0.5 ml CDCl₃
diallylamine hydrochloride

    Assign.     Shift(ppm)

      A             9.8
      B             6.072
      C             5.555
      D             5.404
      E             3.61

     Hz     ppm     Int.

    878.44   9.809    111
    567.69   6.339    105
    560.94   6.264    236
    557.88   6.230    139
    554.38   6.191    113
    551.25   6.156    329
    550.44   6.147    242
    544.88   6.084    157
    543.63   6.071    481
    540.56   6.036    256
    536.94   5.996    227
    533.94   5.962    594
    527.44   5.890    302
    502.44   5.611    181
    501.25   5.597    586
    499.88   5.582   1000
    498.81   5.570    443
    495.25   5.530    872
    494.44   5.521    629
    493.88   5.515    539
    486.63   5.434    287
    485.56   5.422    623
    484.06   5.405    557
    483.38   5.398    484
    482.56   5.389    609
    481.50   5.377    271
    325.75   3.638    479
    325.44   3.634    482
    325.06   3.630    481
    322.63   3.603    461
    321.38   3.589    469
    320.75   3.582    477

KBr disc