8-甲基喹啉(611-32-5)紅外圖譜(IR1)
InChI:InChI=1S/C10H9N/c1-8-4-2-5-9-6-3-7-11-10(8)9/h2-7H,1H3
InChIKey: JRLTTZUODKEYDH-UHFFFAOYSA-N
Smiles:N1C2C(=CC=CC=2C)C=CC=1
-
Mass
MS-NW-0148
8-methylquinoline
C10H9N (Mass of molecular ion: 143)
Source Temperature: 220 °C
Sample Temperature: 75 °C
Reservoir, 75 eV
38.0 1.5
39.0 5.5
50.0 2.8
51.0 3.9
52.0 1.1
58.5 5.6
62.0 2.9
63.0 6.9
64.0 1.8
65.0 2.1
70.5 4.7
71.5 4.2
74.0 1.6
75.0 2.0
76.0 1.4
77.0 1.1
87.0 1.4
88.0 1.7
89.0 6.4
90.0 2.0
113.0 1.9
114.0 3.1
115.0 14.3
116.0 6.2
117.0 5.6
140.0 2.5
141.0 8.1
142.0 43.2
143.0 100.0
144.0 11.1
90 MHz in CDCl3
400 MHz in CDCl3
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| 1H NMR |
89.56 MHz |
| C10 H9 N
|
0.025 g : 0.5 ml CDCl3
|
| 8-methylquinoline
|
 |
Assign. Shift(ppm)
A 8.939
B 8.106
C 7.64
D 7.57
E 7.44
F 7.38
G 2.825
J(A,B)=1.8HZ. J(A,F)=4.2HZ. J(B,F)=8.3HZ.
|
Hz ppm Int.
803.75 8.975 116
801.94 8.955 125
799.56 8.928 124
797.75 8.908 126
731.44 8.168 119
729.63 8.147 114
723.13 8.075 151
721.31 8.054 139
690.38 7.709 54
688.44 7.687 56
682.88 7.625 104
682.38 7.620 99
680.75 7.602 168
675.19 7.539 162
674.44 7.531 159
672.06 7.505 74
670.13 7.483 286
666.25 7.440 164
662.81 7.401 198
657.94 7.347 127
655.69 7.322 48
653.75 7.300 115
649.56 7.253 88
252.94 2.825 1000
-
| 1H NMR |
399.65 MHz |
| C10 H9 N
|
0.025 g : 0.5 ml CDCl3
|
| 8-methylquinoline
|
|
Assign. Shift(ppm)
A 8.949
B 8.120
C 7.653
D 7.560
E 7.432
F 7.386
G 2.826
J(A,B)=1.7HZ. J(A,F)=4.2HZ. J(B,F)=8.3HZ. J(C,E)=8.1HZ. J(D,E)=7.1HZ.
|
Hz ppm Int.
3579.83 8.958 130
3578.13 8.954 142
3575.68 8.948 146
3573.85 8.943 151
3250.37 8.134 141
3248.66 8.129 151
3242.07 8.113 152
3240.36 8.108 159
3063.48 7.666 104
3062.99 7.665 104
3055.42 7.646 126
3054.81 7.644 126
3026.61 7.574 77
3025.51 7.571 98
3024.29 7.568 85
3023.32 7.565 43
3020.51 7.558 46
3019.53 7.556 106
3018.55 7.553 131
3017.33 7.550 106
3016.36 7.548 52
2977.17 7.450 161
2970.09 7.432 139
2969.12 7.430 156
2962.04 7.412 108
2957.76 7.401 181
2953.61 7.391 181
2949.58 7.381 173
2945.31 7.370 170
1129.64 2.827 1000