甲基三丁基氯化銨(56375-79-2)質(zhì)譜(MS)

產(chǎn)品名稱:甲基三丁基氯化銨

CAS:56375-79-2

分子式:C13H30ClN

分子量: 235.84

Mass

MS-NW-8620          
tributylmethylammonium chloride
C13H30ClN           (Mass of molecular ion:    235)

   Source Temperature: 260 °C
   Sample Temperature: 140 °C
   Direct, 75 eV

      15.0       2.9
      27.0       8.3
      28.0       4.8
      29.0      19.1
      30.0       7.1
      36.0       1.0
      39.0       3.9
      41.0      26.2
      42.0      11.0
      43.0      12.9
      44.0      29.2
      49.0       1.6
      50.0      12.4
      52.0       4.0
      55.0       5.5
      56.0      27.1
      57.0      13.3
      58.0      35.2
      59.0       1.3
      63.0       1.1
      70.0       2.3
      72.0       1.4
      84.0       3.1
      86.0       4.2
      98.0       4.2
     100.0     100.0
     101.0       7.2
     128.0       1.2
     142.0      95.9
     143.0      17.7
     144.0       1.5
     185.0       7.0
     186.0       1.1
     200.0       1.0

400 MHz in CDCl3

¹H NMR	399.65 MHz
C₁₃ H₃₀ Cl N	0.04 ml : 0.5 ml CDCl₃
tributylmethylammonium chloride

    Assign.     Shift(ppm)

      A             3.429
      B             3.279
      C             1.699
      D             1.449
      E             1.003

     Hz     ppm     Int.

   1379.39   3.452    238
   1374.15   3.439    165
   1373.90   3.438    165
   1370.85   3.431    200
   1362.30   3.409    251
   1310.55   3.280    485
    695.07   1.740     68
    687.74   1.721    134
    683.11   1.710    137
    679.20   1.700    180
    675.17   1.690    130
    671.26   1.680    141
    663.21   1.660     67
    596.44   1.493     52
    589.11   1.475    164
    581.67   1.456    269
    574.22   1.437    257
    566.89   1.419    142
    559.45   1.400     38
    408.33   1.022    556
    401.00   1.004   1000
    396.97   0.994     96
    393.55   0.985    436

in CDCl3