5455-98-1

N-(2,3-環(huán)氧丙基)鄰苯二甲酰胺(5455-98-1)質譜(MS)

產品名稱:N-(2,3-環(huán)氧丙基)鄰苯二甲酰胺

CAS:5455-98-1

分子式:C11H9NO3

分子量: 203.19

InChI:InChI=1S/C11H9NO3/c13-10-8-3-1-2-4-9(8)11(14)12(10)5-7-6-15-7/h1-4,7H,5-6H2

InChIKey: DUILGEYLVHGSEE-UHFFFAOYSA-N

Smiles:C1(=O)C2=C(C=CC=C2)C(=O)N1CC1CO1

Mass

MS-NW-6540          
N-(2,3-epoxypropyl)phthalimide
C11H9NO3            (Mass of molecular ion:    203)

   Source Temperature: 140 °C
   Sample Temperature: 110 °C
   Direct, 75 eV

      15.0       4.2
      17.0       1.0
      18.0       4.5
      26.0       1.5
      27.0       5.5
      28.0       2.7
      29.0       4.0
      31.0       2.7
      37.0       1.4
      38.0       2.9
      39.0       3.6
      40.0       1.4
      41.0       1.1
      42.0       2.1
      43.0       5.7
      49.0       1.2
      50.0      23.5
      51.0       9.5
      52.0       4.1
      53.0       1.0
      55.0       1.0
      56.0       1.8
      62.0       1.5
      63.0       3.0
      64.0       2.0
      65.0       1.0
      66.0       2.9
      70.0       2.3
      73.0       1.4
      74.0       8.9
      75.0      12.0
      76.0      41.9
      77.0      28.4
      78.0       3.0
      89.0       4.4
      90.0       6.0
      91.0       1.9
     102.0       7.6
     103.0       7.7
     104.0      33.0
     105.0      15.9
     106.0       1.9
     116.0       2.1
     117.0      12.5
     118.0       3.1
     119.0       1.1
     128.0       1.5
     129.0       3.6
     130.0      11.7
     131.0       1.5
     132.0       7.9
     133.0      14.8
     134.0       1.5
     144.0       1.5
     145.0      10.3
     146.0       9.8
     147.0       5.4
     148.0       1.3
     157.0       1.4
     159.0      28.3
     160.0     100.0
     161.0      52.3
     162.0       5.5
     172.0       2.4
     173.0       4.5
     174.0      12.4
     175.0       5.7
     185.0       5.5
     186.0       1.1
     203.0       7.4
     204.0       1.1

90 MHz in CDCl3

¹H NMR	89.56 MHz
C₁₁ H₉ N O₃	0.043 g : 0.5 ml CDCl₃
N-(2,3-epoxypropyl)phthalimide

    Assign.     Shift(ppm)

      A             7.85
      B             7.75
      C     *1      3.95
      D     *1      3.81
      E             3.238
      F             2.80
      G             2.690
     
     J(C,D)=14.2HZ. J(F,G)=4.9HZ. J(E,G)=2.5HZ. J(E,F)=3.9HZ.
     J(C,E)=J(D,E)=4.9HZ.

     Hz     ppm     Int.

    709.88   7.927    359
    708.19   7.908     50
    707.19   7.897    225
    706.00   7.883    313
    705.19   7.874    284
    703.44   7.855    569
    701.31   7.831    877
    700.81   7.826   1000
    699.56   7.812    533
    697.50   7.789    393
    696.50   7.777    960
    696.00   7.772    987
    693.88   7.748    459
    692.81   7.736    112
    692.13   7.729    293
    691.31   7.719    329
    690.13   7.706    242
    687.38   7.676    378
    367.06   4.099     64
    362.00   4.042     78
    352.88   3.941    354
    350.19   3.911     49
    347.25   3.878    715
    344.63   3.849     55
    344.19   3.844     59
    342.31   3.823    596
    332.88   3.717     89
    328.00   3.663    126
    298.13   3.329    106
    295.63   3.301    118
    294.31   3.287    140
    293.31   3.276    145
    291.75   3.258    151
    290.69   3.246    160
    289.50   3.233    188
    288.19   3.218     94
    286.88   3.204    190
    285.69   3.190    102
    284.31   3.175    110
    281.75   3.146    103
    256.13   2.860    174
    255.69   2.855    173
    251.25   2.806    391
    250.88   2.802    390
    247.38   2.763    328
    247.00   2.758    323
    243.75   2.722    496
    241.19   2.694    468
    238.88   2.668    239
    236.31   2.639    202

in CDCl3