4975-73-9

N,N'-二環(huán)己基-4-嗎啉脒(4975-73-9)紅外圖譜(IR2)

產(chǎn)品名稱:N,N'-二環(huán)己基-4-嗎啉脒

CAS:4975-73-9

分子式:C17H31N3O

分子量: 293.45

Mass

MS2014-05050CW      
N,N'-dicyclohexyl-4-morpholinecarboxamidine
C17H31N3O           (Mass of molecular ion:    293)

   Source Temperature: 240 °C
   Sample Temperature:  20 °C
   Direct, 70 eV

      17.0       2.3
      18.0      10.7
      27.0       5.5
      28.0       8.5
      29.0      10.5
      30.0       7.4
      39.0       7.5
      40.0       1.3
      41.0      49.6
      42.0      15.9
      43.0      44.4
      44.0       7.7
      45.0      11.6
      53.0       7.0
      54.0       9.5
      55.0      75.0
      56.0      28.4
      57.0      16.2
      58.0       5.5
      59.0       1.1
      60.0       1.7
      65.0       1.3
      66.0       1.0
      67.0       9.9
      68.0       6.3
      69.0      43.6
      70.0       6.5
      71.0       2.8
      72.0       9.3
      73.0       4.0
      74.0       1.0
      77.0       1.6
      79.0       5.3
      80.0       2.9
      81.0      20.6
      82.0       9.8
      83.0      36.6
      84.0      12.8
      85.0       5.5
      86.0      42.5
      87.0      17.5
      88.0       7.9
      94.0       1.6
      95.0       4.5
      96.0       5.0
      97.0       6.1
      98.0      90.9
      99.0      47.5
     100.0       4.3
     101.0      10.5
     102.0       1.4
     107.0       1.0
     108.0       1.7
     109.0       3.0
     110.0     100.0
     111.0      10.3
     112.0       4.4
     113.0      59.2
     114.0       9.5
     115.0       4.5
     121.0       1.1
     122.0       1.3
     123.0       5.9
     124.0       6.2
     125.0      32.7
     126.0       9.3
     127.0      10.1
     128.0       3.2
     129.0      19.1
     130.0      14.3
     131.0       1.0
     136.0       1.6
     137.0       1.7
     138.0       5.3
     139.0       6.4
     140.0       6.7
     141.0       3.7
     142.0       1.6
     150.0       1.0
     151.0       3.4
     152.0       4.1
     153.0      37.3
     154.0      25.1
     155.0       4.1
     156.0       1.4
     163.0       3.2
     164.0       2.1
     165.0       5.3
     166.0      10.3
     167.0       6.1
     168.0      13.0
     169.0       3.0
     177.0       1.3
     178.0       1.8
     179.0       1.5
     180.0       6.5
     181.0      15.8
     182.0       5.9
     183.0       3.6
     192.0       1.9
     193.0       3.2
     194.0       5.0
     195.0       8.1
     196.0      14.4
     197.0       2.8
     206.0       2.2
     207.0       7.9
     208.0      17.3
     209.0       3.8
     210.0       4.3
     211.0      27.8
     212.0      10.1
     213.0       1.2
     220.0       4.8
     221.0       2.0
     222.0      29.4
     223.0       9.1
     224.0       1.6
     234.0       2.1
     236.0      16.1
     237.0       4.6
     238.0       2.6
     248.0       7.7
     249.0       1.9
     250.0      85.7
     251.0      14.7
     252.0       2.3
     262.0       2.1
     263.0       4.7
     264.0       7.6
     265.0       1.9
     278.0       2.1
     290.0       2.1
     292.0       6.0
     293.0      33.8
     294.0       7.4

400 MHz in CDCl3

¹H NMR	399.65 MHz
C₁₇ H₃₁ N₃ O	0.040 g : 0.5 ml CDCl₃
N,N'-dicyclohexyl-4-morpholinecarboxamidine

    Assign.     Shift(ppm)

      A             3.675
      B             3.079
      C     *1      3.00
      D     *1      2.90
      E     *2      1.91
      F             1.75
      G     *2   1.65 to 1.55
      J     *3      1.33
      K             1.29
      L             1.19
      M     *3      1.062
     
     ASSIGNED BY H-H AND C-H COSY.

     Hz     ppm     Int.

   1473.88   3.688    805
   1469.24   3.677   1000
   1464.48   3.665    909
   1235.47   3.092    778
   1230.59   3.080    929
   1225.95   3.068    772
   1217.29   3.046     33
   1211.67   3.032     50
   1207.89   3.023     81
   1203.86   3.013     62
   1201.05   3.006     90
   1197.27   2.996    150
   1193.48   2.987     96
   1190.55   2.979     66
   1186.52   2.969     86
   1183.11   2.961     52
   1182.74   2.960     52
   1172.73   2.935     30
   1169.19   2.926     68
   1168.82   2.925     68
   1165.04   2.916     86
   1163.57   2.912     87
   1161.87   2.908     81
   1159.30   2.901    129
   1155.40   2.892    112
   1150.88   2.880     57
   1149.29   2.876     66
   1145.51   2.867     44
    769.29   1.925    172
    766.72   1.919    187
    762.57   1.909    128
    762.08   1.907    129
    761.72   1.906    128
    757.08   1.895    198
    756.10   1.892    194
    754.15   1.888    200
    704.71   1.764    413
    701.66   1.756    307
    700.68   1.754    306
    700.20   1.753    305
    694.95   1.739    355
    691.77   1.731    356
    655.52   1.641    114
    650.88   1.629    161
    647.71   1.621    187
    638.67   1.599    284
    636.60   1.593    295
    636.11   1.592    294
    630.49   1.578    203
    629.76   1.576    201
    625.37   1.565    286
    617.19   1.545     32
    612.06   1.532     30
    611.69   1.531     30
    550.90   1.379     59
    539.18   1.350    202
    536.38   1.343    198
    527.95   1.322    460
    524.17   1.312    358
    520.14   1.302    459
    510.74   1.278    346
    508.18   1.272    347
    506.84   1.269    419
    501.95   1.256    119
    498.54   1.248    192
    495.73   1.241    182
    489.14   1.224     76
    487.30   1.220     70
    481.69   1.206    159
    478.64   1.198    126
    472.41   1.183    131
    469.36   1.175    196
    460.82   1.154     84
    460.57   1.153     84
    457.28   1.145    123
    454.22   1.137     71
    448.49   1.123     33
    442.50   1.108    102
    439.33   1.100     96
    436.28   1.092     38
    430.05   1.077    200
    427.73   1.071    195
    419.31   1.050    180
    416.63   1.043    183
    410.77   1.028     36
    407.71   1.021     69
    404.42   1.012     66
    404.17   1.012     66

in CDCl3