2-(2-噻吩)吡啶(3319-99-1)核磁圖(1HNMR)
InChI:InChI=1S/C9H7NS/c1-2-6-10-8(4-1)9-5-3-7-11-9/h1-7H
InChIKey: QLPKTAFPRRIFQX-UHFFFAOYSA-N
Smiles:C1(C2SC=CC=2)=NC=CC=C1
-
Mass
MS-NW-7147
2-(2-thienyl)pyridine
C9H7NS (Mass of molecular ion: 161)
Source Temperature: 240 °C
Sample Temperature: 180 °C
Reservoir, 75 eV
26.0 1.3
27.0 1.5
28.0 2.1
37.0 1.2
38.0 2.2
39.0 7.1
45.0 6.9
50.0 5.1
51.0 9.2
52.0 4.6
57.0 1.3
58.0 3.8
58.5 2.5
61.0 1.1
62.0 2.2
63.0 5.3
64.0 1.5
67.0 1.4
69.0 3.9
74.0 1.7
75.0 2.1
76.0 1.7
77.0 1.3
78.0 8.4
79.0 1.2
80.0 2.1
80.5 4.2
81.0 1.3
82.0 2.1
83.0 1.1
89.0 7.6
90.0 4.8
91.0 1.3
93.0 1.0
104.0 2.2
108.0 2.9
109.0 1.5
116.0 6.1
117.0 16.6
118.0 1.6
121.0 1.1
122.0 1.7
128.0 9.6
129.0 1.5
133.0 1.6
134.0 4.6
135.0 5.7
159.0 1.1
160.0 25.1
161.0 100.0
162.0 11.7
163.0 5.2
400 MHz in CDCl3
90 MHz in CDCl3
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| 1H NMR |
399.65 MHz |
| C9 H7 N S
|
0.047 g : 0.5 ml CDCl3
|
| 2-(2-thienyl)pyridine
|
 |
Assign. Shift(ppm)
A 8.559
B 7.65
C 7.64
D 7.565
E 7.382
F 7.12
G 7.098
J(A,F) = 4.6 HZ.
J(D,G) = 3.8 HZ.
J(D,E) = 1.3 HZ.
J(E,G) = 5.1 HZ.
J(B,F) = 6.2 HZ.
J(C,F) = 2.3 HZ.
|
Hz ppm Int.
3428.22 8.579 33
3424.19 8.568 310
3423.10 8.566 357
3422.61 8.565 374
3421.51 8.562 326
3419.31 8.556 318
3417.97 8.553 478
3416.50 8.549 305
3414.06 8.543 30
3069.46 7.681 35
3067.14 7.675 169
3065.43 7.671 162
3063.84 7.667 57
3063.23 7.665 61
3062.50 7.663 64
3060.91 7.659 97
3059.08 7.655 631
3057.37 7.651 656
3054.57 7.644 665
3053.47 7.641 769
3052.86 7.639 949
3052.12 7.637 864
3051.27 7.635 1000
3046.51 7.623 177
3045.41 7.621 164
3044.19 7.618 71
3042.85 7.614 55
3041.87 7.612 39
3041.14 7.610 37
3026.00 7.572 756
3024.90 7.569 762
3022.34 7.563 765
3021.12 7.560 771
2953.00 7.389 736
2951.78 7.386 706
2949.58 7.381 68
2947.88 7.377 780
2946.78 7.374 774
2854.49 7.143 42
2851.44 7.135 398
2849.12 7.130 351
2847.66 7.126 91
2846.56 7.123 400
2845.21 7.120 386
2843.99 7.117 385
2842.77 7.114 393
2840.94 7.109 944
2840.45 7.108 471
2837.89 7.101 442
2837.28 7.100 899
2835.94 7.097 829
2832.28 7.087 765
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| 1H NMR |
89.56 MHz |
| C9 H7 N S
|
0.043 g : 0.5 ml CDCl3
|
| 2-(2-thienyl)pyridine
|
|
Assign. Shift(ppm)
A 8.55
B 7.67
C 7.62
D 7.57
E 7.371
F 7.11
G 7.10
|
Hz ppm Int.
769.88 8.597 181
768.38 8.580 253
767.06 8.565 198
765.06 8.543 206
763.69 8.528 328
762.25 8.512 191
687.44 7.676 442
685.81 7.658 761
684.75 7.646 470
682.38 7.620 1000
681.00 7.604 819
679.94 7.593 543
678.75 7.579 560
676.25 7.551 536
675.13 7.539 578
672.88 7.514 69
663.75 7.412 410
662.56 7.398 388
660.31 7.373 79
658.63 7.355 625
657.44 7.341 518
643.19 7.182 273
639.13 7.137 792
638.31 7.128 463
637.19 7.115 124
635.50 7.096 655
634.06 7.080 639
630.38 7.039 450
629.75 7.032 221