二戊胺(2050-92-2)核磁圖(¹HNMR)

產(chǎn)品名稱:二戊胺

CAS:2050-92-2

分子式:C10H23N

分子量: 157.3

InChI:InChI=1S/C10H23N/c1-3-5-7-9-11-10-8-6-4-2/h11H,3-10H2,1-2H3

InChIKey: JACMPVXHEARCBO-UHFFFAOYSA-N

Smiles:C(NCCCCC)CCCC

Mass

MS-NW-8360          
dipentylamine
C10H23N             (Mass of molecular ion:    157)

   Source Temperature: 250 °C
   Sample Temperature: 120 °C
   Reservoir, 75 eV

      27.0       5.2
      28.0       4.1
      29.0       8.6
      30.0      37.1
      39.0       2.8
      41.0      11.3
      42.0       3.9
      43.0      31.0
      44.0      79.9
      45.0       2.6
      55.0       2.3
      56.0       3.3
      57.0       1.6
      69.0       1.9
      70.0       2.9
      71.0       2.5
      86.0       2.0
      98.0       1.4
     100.0     100.0
     101.0       7.0
     156.0       1.0
     157.0       5.4
     158.0       1.0

90 MHz in CDCl3

¹H NMR	89.56 MHz
C₁₀ H₂₃ N	0.04 ml : 0.5 ml CDCl₃
dipentylamine

    Assign.     Shift(ppm)

      A             2.576
      B             1.48
      C          1.41 to 1.23
      D             0.899

     Hz     ppm     Int.

    238.81   2.667    160
    236.44   2.641     96
    235.81   2.633    101
    235.19   2.627     99
    232.00   2.591    351
    231.88   2.590    351
    228.00   2.546     61
    224.88   2.511    287
    142.50   1.592     56
    139.75   1.561    118
    137.81   1.539     78
    136.38   1.523     97
    134.88   1.507    144
    132.38   1.479    212
    130.38   1.456    147
    127.75   1.427    190
    126.50   1.413    234
    125.88   1.406    230
    124.69   1.393    205
    121.94   1.362    572
    120.44   1.345    484
    119.75   1.338    491
    117.88   1.317    462
    115.63   1.292    440
    112.13   1.253    276
    110.00   1.229    338
    104.63   1.169     63
    103.88   1.160     56
     87.56   0.978    165
     85.88   0.959    269
     80.31   0.897   1000
     74.31   0.830    185
     73.56   0.822    173
     71.06   0.794     58
     70.38   0.786     68

in CDCl3