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120-12-7

蒽(120-12-7)ESR圖譜

產(chǎn)品名稱:蒽

CAS:120-12-7

分子式:C14H10

分子量: 178.23

InChI:InChI=1S/C14H10/c1-2-6-12-10-14-8-4-3-7-13(14)9-11(12)5-1/h1-10H

InChIKey: MWPLVEDNUUSJAV-UHFFFAOYSA-N

Smiles:C1=C2C(C=C3C(=C2)C=CC=C3)=CC=C1

  • 圖譜
    Mass 

    MS-NW-0132          
anthracene
C14H10              (Mass of molecular ion:    178)


       Source Temperature: 140 °C
   Sample Temperature:   0 °C
   Direct, 75 eV


          39.0       1.1
      50.0       1.3
      51.0       1.3
      62.0       1.3
      63.0       2.9
      74.0       2.2
      75.0       3.0
      76.0       6.2
      86.0       1.0
      87.0       1.7
      88.0       4.4
      89.0       7.6
      89.5       1.0
      98.0       1.2
     126.0       1.5
     139.0       2.1
     150.0       4.2
     151.0       6.3
     152.0       6.9
     166.0       1.2
     167.0       7.5
     168.0       1.0
     174.0       1.3
     175.0       2.0
     176.0      14.1
     177.0       8.0
     178.0     100.0
     179.0      15.7
     180.0       1.5

90 MHz in CDCl3

  • 圖譜

    1H NMR 89.56 MHz
    C14 H10 saturated in CDCl3
    anthracene
    ChemicalStructure 
        Assign.     Shift(ppm)
    
      A             8.397
      B             7.980
      C             7.440
  

         Hz     ppm     Int.


        752.19   8.399    818
    722.25   8.065    113
    720.00   8.040    469
    716.75   8.004    450
    713.50   7.967    474
    710.31   7.932    624
    707.56   7.901    159
    674.13   7.528    160
    673.75   7.523    162
    670.88   7.491   1000
    667.81   7.457    535
    664.31   7.418    613
    661.06   7.382    731
    658.75   7.356    144

in CDCl3

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KBr disc

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nujol mull

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ANION RADICAL, RED. WITH NA IN THF AND (C4H9)4NCLO4

ANION RADICAL, REDUCTION WITH NA IN THF

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