三氯苯基錫(1124-19-2)紅外圖譜(IR1)

產(chǎn)品名稱:三氯苯基錫

CAS:1124-19-2

分子式:C6H5Cl3Sn

分子量: 302.17

InChI:InChI=1S/C6H5.3ClH.Sn/c1-2-4-6-5-3-1;;;;/h1-5H;3*1H;/q;;;;+3/p-3

InChIKey: UBOGEXSQACVGEC-UHFFFAOYSA-K

Smiles:[Sn](Cl)(Cl)(Cl)C1=CC=CC=C1

¹HNMR

¹³CNMR

IR1

Mass

MS-NW-9653          
trichloro(phenyl)stannane
C6H5Cl3Sn           (Mass of molecular ion:    302)

   Source Temperature: 270 °C
   Sample Temperature: 150 °C
   Reservoir, 75 eV

      18.0       1.8
      27.0       1.4
      28.0       1.4
      35.0       1.1
      36.0       2.3
      38.0       1.6
      39.0       4.4
      50.0      10.5
      51.0      23.8
      52.0       8.3
      57.0       3.2
      63.0       2.3
      74.0       4.2
      75.0       3.4
      76.0       8.1
      77.0      54.5
      78.0      61.4
      79.0       4.1
     112.0     100.0
     113.0       7.1
     114.0      33.1
     115.0       3.8
     116.0       3.5
     117.0       2.2
     118.0       6.1
     119.0       2.7
     120.0       8.3
     122.0       1.1
     124.0       1.4
     126.0       1.2
     127.0       1.3
     128.0       1.8
     143.0       1.5
     145.0       2.0
     147.0       1.4
     149.0       1.5
     150.0       1.3
     151.0      16.2
     152.0      15.6
     153.0      32.1
     154.0      69.2
     155.0      44.7
     156.0       8.4
     157.0      16.9
     158.0       6.5
     159.0       8.4
     161.0       2.1
     186.0       2.0
     187.0       1.1
     188.0       4.7
     189.0       2.0
     190.0       6.8
     191.0       1.0
     192.0       3.8
     193.0       1.5
     194.0       2.1
     195.0       2.4
     196.0       1.5
     197.0       3.8
     198.0       1.0
     199.0       3.2
     201.0       2.1
     228.0       2.7
     229.0       1.7
     230.0       5.3
     231.0       2.5
     232.0       7.6
     233.0       1.2
     234.0       3.2
     236.0       1.8
     263.0       5.4
     264.0       3.1
     265.0      12.3
     266.0       5.7
     267.0      18.3
     268.0       3.9
     269.0      10.8
     270.0       1.2
     271.0       4.7
     273.0       1.9
     298.0       2.1
     299.0       1.2
     300.0       5.3
     301.0       2.7
     302.0       8.4
     303.0       2.1
     304.0       6.2
     305.0       3.2
     306.0       4.7
     307.0       5.7
     308.0       4.3
     309.0       7.5
     310.0       2.2
     311.0       3.8
     313.0       2.2
     342.0       1.7
     344.0       2.8
     346.0       2.3
     348.0       1.6

400 MHz in CDCl3

¹H NMR	399.65 MHz
C₆ H₅ Cl₃ Sn	0.05 ml : 0.5 ml CDCl₃
trichloro(phenyl)stannane

    Assign.     Shift(ppm)

      A          7.61 to 7.56

     Hz     ppm     Int.

   3101.68   7.761     39
   3099.24   7.755     38
   3098.39   7.753     47
   3096.07   7.747     48
   3060.42   7.658     34
   3056.40   7.648     57
   3055.05   7.645     65
   3052.25   7.638    115
   3051.15   7.635    111
   3049.93   7.632    151
   3048.46   7.628    218
   3046.14   7.623    278
   3044.19   7.618    429
   3042.60   7.614    251
   3040.77   7.609    447
   3038.33   7.603    631
   3037.11   7.600   1000
   3035.28   7.595    650
   3034.42   7.593    438
   3032.47   7.588    339
   3031.13   7.585    779
   3030.52   7.583    811
   3025.63   7.571    402
   3025.02   7.570    397
   3023.19   7.565    270
   3021.12   7.560    133
   3018.19   7.553    122
   3017.33   7.550    152
   3015.01   7.545     91
   3009.16   7.530     62
   3007.08   7.525     63
   3002.56   7.513     45
   3001.22   7.510     61
   3000.00   7.507     63
   2993.90   7.492     35
   2992.80   7.489     43
   2986.82   7.474     40
   2985.35   7.470     52
   2984.25   7.468     54
   2982.79   7.464     52

in CDCl3