4-二甲氨基苯甲酸乙酯(10287-53-3)Raman光譜

產品名稱:4-二甲氨基苯甲酸乙酯

CAS:10287-53-3

分子式:C11H15NO2

分子量: 193.24

InChI:InChI=1S/C11H15NO2/c1-4-14-11(13)9-5-7-10(8-6-9)12(2)3/h5-8H,4H2,1-3H3

InChIKey: FZUGPQWGEGAKET-UHFFFAOYSA-N

Smiles:C(OCC)(=O)C1=CC=C(N(C)C)C=C1

Mass

MS-NW-6830          
ethyl p-(dimethylamino)benzoate
C11H15NO2           (Mass of molecular ion:    193)

   Source Temperature: 260 °C
   Sample Temperature: 190 °C
   Reservoir, 75 eV

      15.0       1.7
      18.0       1.6
      26.0       1.0
      27.0       3.5
      28.0       1.7
      29.0       2.7
      39.0       2.3
      42.0       9.9
      43.0       1.3
      44.0       2.3
      50.0       3.6
      51.0       3.8
      52.0       1.5
      58.5       1.6
      59.5       2.4
      63.0       3.0
      64.0       1.2
      65.0       3.1
      66.0       1.0
      73.5      10.4
      74.0       5.1
      75.0       1.6
      76.0       3.1
      77.0      10.9
      78.0       4.9
      79.0       5.0
      90.0       2.2
      91.0       4.2
      92.0       2.4
      93.0       1.5
     103.0       1.6
     104.0       6.6
     105.0       8.0
     106.0       1.1
     118.0       4.1
     119.0       4.3
     120.0       8.2
     121.0       6.3
     132.0       3.5
     148.0     100.0
     149.0      13.8
     150.0       2.1
     164.0      41.6
     165.0      24.4
     166.0       2.6
     178.0       1.3
     192.0      12.7
     193.0      92.6
     194.0      11.9
     195.0       1.3

400 MHz in CDCl3

¹H NMR	399.65 MHz
C₁₁ H₁₅ N O₂	0.040 g : 0.5 ml CDCl₃
ethyl p-(dimethylamino)benzoate

    Assign.     Shift(ppm)

      A             7.911
      B             6.630
      C             4.315
      D             3.015
      E             1.360

     Hz     ppm     Int.

   3169.07   7.930     22
   3166.26   7.923    175
   3164.18   7.918     55
   3159.30   7.906     58
   3157.10   7.900    179
   3154.30   7.893     22
   2657.35   6.650     21
   2654.42   6.642    155
   2652.34   6.637     49
   2647.46   6.625     50
   2645.39   6.620    149
   1735.47   4.343     63
   1728.27   4.325    187
   1721.19   4.307    191
   1714.11   4.290     65
   1204.96   3.016   1000
    550.66   1.378    197
    543.46   1.360    371
    536.38   1.343    193

in CDCl3